Volume 37 Issue 3
Sep.  2023
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FENG Rumeng, LIANG Wei, CHEN Lu, YANG Shixin, DENG Ruyi, ZHANG Xiaoqing, LI Wenyao. Effect of citric acid on catalytic activity of molybdenum disulfide catalyst for hydrogen evolution reaction[J]. Journal of Shanghai University of Engineering Science, 2023, 37(3): 305-310. doi: 10.12299/jsues.22-0340
Citation: FENG Rumeng, LIANG Wei, CHEN Lu, YANG Shixin, DENG Ruyi, ZHANG Xiaoqing, LI Wenyao. Effect of citric acid on catalytic activity of molybdenum disulfide catalyst for hydrogen evolution reaction[J]. Journal of Shanghai University of Engineering Science, 2023, 37(3): 305-310. doi: 10.12299/jsues.22-0340

Effect of citric acid on catalytic activity of molybdenum disulfide catalyst for hydrogen evolution reaction

doi: 10.12299/jsues.22-0340
  • Received Date: 2022-11-15
  • Accepted Date: 2022-11-15
  • Publish Date: 2023-09-30
  • Thioacetamide with stable properties and strong reducing ability was selected as sulfur source and reducing agent to prepare MoS2 catalyst by simple hydrothermal method. The influence of different amounts of citric acid on its electrochemical performance was investigated. The morphology and microstructure were characterized by SEM and TEM, electrochemical methods including CV, LSV and Tafel were used for characterization. The results show that the addition of citric acid could increase the electrochemical active surface area of MoS2 catalyst and enhance the hydrogen evolution reaction (HER) catalytic activity of MoS2 catalyst.
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  • [1]
    葛静敏. 二硫化钼的电子结构调控及其电化学析氢性能研究[D]. 北京: 北京化工大学, 2021.
    [2]
    关雨萌, 牛亚楠, 姚婉婷. 硫化物催化剂电催化析氢性能的研究进展[J] . 辽宁化工,2021,50(5):644 − 646.
    [3]
    LI Y G, WANG H L, XIE L M, et al. MoS2 nanoparticles grown on graphene: An advanced catalyst for the hydrogen evolution reaction[J] . Journal of the American Chemical Society,2011,133(19):7296 − 7299. doi: 10.1021/ja201269b
    [4]
    WANG Q H, KALANTAE-ZADENH K, KIS A, et al. Electronics and optoelectronics of two-dimensional transition metal dichalcogenides[J] . Nature Nanotechnology,2012,7(11):699 − 712. doi: 10.1038/nnano.2012.193
    [5]
    李琬卉. 石墨双炔类材料薄膜的制备及其光电性质研究[D]. 天津: 天津大学, 2020.
    [6]
    吕宪伟, 胡忠攀, 赵挥, 等. 自支撑型过渡金属磷化物电催化析氢反应研究[J] . 化学进展,2018,30(7):947 − 957.
    [7]
    郭胜平, 吴伟端. 原位聚合PS/纳米MoS2复合材料的制备及其性能[J] . 玻璃钢/复合材料,2006(2):34 − 36.
    [8]
    朱敏, 张招柱, 王坤, 等. 二硫化钼填充聚酰亚胺复合材料的摩擦学性能[J] . 高分子材料科学与工程,2005(5):232 − 238.
    [9]
    程美美. 石墨烯和二硫化钼修饰电极的电化学检测及析氢效应研究[D]. 西安: 西北大学, 2017.
    [10]
    温月丽. 纳米Cu及CuAl复合物的可规模化制备研究[D]. 太原: 太原理工大学, 2012.
    [11]
    贾晓峰. 一维二硫化钼纳米结构的制备及其光电和气敏性能的研究[D]. 兰州: 兰州大学, 2021.
    [12]
    HU C L, ZHANG L, GONG J L. Recent progress made in the mechanism comprehension and design of electrocatalysts for alkaline water splitting[J] . Energy & Environmental Science,2019:2620 − 2645.
    [13]
    樊梅红. 过渡金属化合物/碳复合材料的设计合成与电催化水裂解析氢性能研究[D]. 长春: 吉林大学, 2019.
    [14]
    李席涛. 金属相MoS2基催化剂的设计制备及光/电催化性能研究[D]. 北京: 北京化工大学, 2021.
    [15]
    谢子杰. 熔盐电解法制备过渡金属(Nb、Cu、Co)掺杂MoS2及其析氢性能研究[D]. 南昌: 东华理工大学, 2021.
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